-16. A novel apparatus has been constructed that is both a hot plate and an anal
ID: 1082720 • Letter: #
Question
-16. A novel apparatus has been constructed that is both a hot plate and an analytical balance to determine how the waters of hydra are driven off from a sample of a hydrate. In this experiment, a 0.822 g sample of copper sulfate pentahydrate is placed in arn evaporating dish that weighs 44.056 g. The hot plate is turned on to a setting of 2 (140°C) and data is recorded for mass as a funct f time as the water is driven off of the original sample. Each time that there is a level reading of mass for more than 2 minutes, th ists a stable compound. Identify the formula for each of the two stable compounds using the graph of the data below. For this problem, your work counts. You must prove what the formulas are based on calculations. Sorry, but no points for guessin Data from Experiment Picture of Hot Plate/Analytical Balance Mass v. Time for Cus04 5H20 on a Hot Plate/Scale 44.75 44.7 44.65 44.35 Time (minExplanation / Answer
Ans: First we have to calculate the relative masses of all the Copper Sulphate.N.hydrate forms.
Let's make a table of observation
Initial mass of Cuvette = 44.056 g
Mass of sample, that has been taken = 0.822 g
Total mass at the beginning of experiment = 44.875g (Cuvette + sample)
Observations: smallest interval on the scale is 0.025g
Here we have observed two sets of masses.
S.no
Total mass (g)
(Cuvette + sample)
Mass of sample after heating (g)
1
44.775
0.719
2
44.575
0.519
We can have five more extra form of Copper sulphate with different masses
CuSO4.5H2O
249.68g
Relative ratio with pentahydrate
CuSO4.4H2O
231.68g
0.92
CuSO4.3H2O
213.68g
0.85
CuSO4.2H2O
195.68g
0.78
CuSO4.H2O
177.68g
0.71
CuSO4
159.68g
0.63
By simply comparing the ratio of masses of other form with starting material, we can conclude the stable phase obtained in the experiment.
Obs 1. mass obtained/ actual mass taken = 0.719/0.822 = 0.87
Obs 2. mass obtained/ actual mass taken = 0.519/0.822 = 0.63
Hence from calculations, we can say that two most stable phases obtained belongs to CuSO4.3H2O and CuSO4.
S.no
Total mass (g)
(Cuvette + sample)
Mass of sample after heating (g)
1
44.775
0.719
2
44.575
0.519
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