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REPORT REACTION TYPES, EQUATIONS AND QUALITATIVE ANALYSIS Student Name Lab Day A

ID: 482994 • Letter: R

Question

REPORT REACTION TYPES, EQUATIONS AND QUALITATIVE ANALYSIS Student Name Lab Day A. Qualitative analysis of known solutions (spot testing) Table 1: Report nal colour, then (i) state either precipitate (ppt) and amount, or colour change (cc), or no reaction (NR) (2 marks) Reagent added Test Solution Test white White WHITE Lead (II) Nitrate yellow White White PPT L CC L PPT s PPT M PPT s S Orange Blood red Yellow orange YELLow YELLow Iron (Ill) Nitrate PPT L PPT S CC L CC L Nickel (II) Nitrate Ni ORANGE Blue PURPLE PINK NR PPT L PPT TL PPT L PPT L Silver (I) Nitrate Blood red WHITE NR BLACK WHITE NR WHITE Barium Nitrate light yellow NR WHITE Negative Control Unknown Sample unknown Sample identity of unknown Cations: H:

Explanation / Answer

The unknown sample # 6 contains Pb^2+ and Ni^2+.

Blue + white ppt

Pb(SCN)4

Ni(SCN)6^2+

CC L purple + white ppt

Ni(NH3)6^2+ (purple)

Pb(NH3)4^2+

red ppt

Ni(DMG)2

white ppt

PbCl2

white ppt

PbSO4

K2CrO4 KSCN NH3 DMG HCl H2SO4 orange ppt of PbCrO4

Blue + white ppt

Pb(SCN)4

Ni(SCN)6^2+

CC L purple + white ppt

Ni(NH3)6^2+ (purple)

Pb(NH3)4^2+

red ppt

Ni(DMG)2

white ppt

PbCl2

white ppt

PbSO4