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Fill in the reaction table below. Make sure you correctly calculate the molar am

ID: 527479 • Letter: F

Question

Fill in the reaction table below. Make sure you correctly calculate the molar amounts of your reactive materials. Calculate the Theoretical Yield of your product, i.e. the mass you would expect to recover (assuming 100% conversion to product). Distinguishing between the products A, B and C is quite challenging by IR spectroscopy alone -explain the differences and similarities that you would expect to see in the corresponding IR spectra. Which functional groups are the same, and which are different?

Explanation / Answer

Filling table for carvone epoxidation

Table of reagents

D-(+)-carvone      C10H14O        1.0 mol-eq       150.22 g/mol         4.73 mmol        0.72 g

6M aq. NaOH       NaOH            0.32 mol-eq       40 g/mol               1.5 mmol           1.0 ml

30% aq H2O2       H2O2              2.8 mol-eq       34 g/mol               13.2 mmol         1.5 ml

MeOH                   MeOH                     -               32 g/mol                      -                  8 ml

Product              C10H14O2         1.0 mol-eq      166.22 g/mol         4.73 mmol         0.79 g

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