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1H NMR (CDC13, 300MHz): chem2400 Mo02C12DMSO2 recrystallized Current Data Parame

ID: 555773 • Letter: 1

Question

1H NMR (CDC13, 300MHz): chem2400 Mo02C12DMSO2 recrystallized Current Data Parameters NAME Moo2C12 (DMSO) 2 chem 2400 EXPNO E2 -Acquisition Paraneters Date Time INSTRUM 20171031 15.04 spect PULPHOG TD SOLVENT NS DS SWH FIDRES COC13 1 6 6188.119 H 0.156258 B .1998415 sec 645 0.800 usec .50 usec ow DE TE D1 TDO 300.0 K 150000000 e e-ees CHANNEL n ".."…- 00-1818537 MH sPO1 NUC P1 PLN 14.52 usec 6.40000010 F2-Processing paraneters SI SF 32768 300.1800079 MIl EM SSH LH .30 Ha PC 1.00 7.5 7.0 6.5 6.05.5 5.0 454.0 3.5 3.0 2.52.0 1.5 .0 0.5 ppm

Explanation / Answer

NMR indicate acetylene compound.

and 2.94 ppm indicate  acetylene hydrogen and other two value shows singlate for aliphatic compound.

but structure not clear , required more data, like mass, and I.R

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