Question
What is the reaction for this experiment? The starting material was ethylbenzene.
Dle spectroscopy. The possible starting materials are toluene, ethylbenzene, and SAFETY AND HAZARDS methoxybenzene (anisole) Wear safety soggles and gloves for this experiment. Aluminum chloride is water corrosive. It will react with the moisture on your skin to liberate HCI, necessary, and work quickly. Acetyl chloride is also corrosive. Be sure to keep it in the sensitive, an irritant, and Handle it with care, weigh out only what hood. Keep all reagent bottles tightly capped. Discard aqueous waste down the drain with lots of water. waste into the appropriate waste containers. Handle syringes or pipettes with care. vringes in the appropriate containers. ganic Do not wash your glassware just before doing this experiment. Your glassware pound not wash your syringe between adding the acetyl chloride and the aromatic com Weigh out the aluminum chloride quickly and keep the container tightly capped. Obtain the IR spectrum as a thin film once you do your reaction. Put the analysis in your lab report. Obtain an NMR spectrum from your TA and include the analysis of NMR in your lab report OCEDURE drous aluminum chloride (3.0 g) and 6.0 mL of methylene chloride are placed into a 25-ml round tomed flask equipged with a stir bar. Attach a Claisen head, septum, cap,and reflux condenser to the lask stir the mixtupewhile cooling in an ice/water bath (DON'T FORGE THE ICE BATH!!!!). Use a drying tube n the top. Note: not all of the aluminum chlogide will dissolve in the mixture. Mix acetyl ch nste.0 ml of methylehe chloride in a scintillation vial. Add the mixture of acetyl chloride/methvlene chlo atic he reaction flask dropwise over 5-10 minuteswith on emovable needle that can pierce the septum to do that addition. ml) and stirring. You may use a plastic syringe equipped with a drying tube wator out clamo rubber water in -Claisen adapter clamp _ round bottom fask 23
Explanation / Answer
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Please alleast provide all of the reagents. Please provide all of the reagents of this experiment then we can say what is the reaction of this experiment.
Provide all of the reagents in my comments box then i can solve your problem. Thank you
