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Calculate the volumes of needed to make solutions of alkaline phosphatase and p-

ID: 61139 • Letter: C

Question

Calculate the volumes of needed to make solutions of alkaline phosphatase and p-nitrophenylphosphate with the given concentration and update the table below.Show one (1) sample calculation.

Reagents:

Reaction buffer: 0.5 M Tris HCl (pH 8.0) with 5 mM MgCl2

Alkaline phosphatase: 500 µg/mL stock solution in reaction buffer.

p-nitrophenylphosphate: 1000 µM and 10,000 µM stock solution in reaction buffer.

A. Enzyme solutions (See lab handout Section A-3 for details.)

#

[Enzyme] ug/mL

Alkaline phosphatase (µL)

Buffer (µL)

Total volume (µL)

1

100

2000

2

125

2000

3

150

2000

#

[Enzyme] ug/mL

Alkaline phosphatase (µL)

Buffer (µL)

Total volume (µL)

1

100

2000

2

125

2000

3

150

2000

Explanation / Answer

1. Alkaline phosphatase stock - 500 ug/ml

Concentration(stock) x Volume(stock) = Concentration(final) x Volume(final)

Volume of stock = 100 ug/ml X 1 ml/ 500 = 0.2 ml

S.No [Enzyme] ug/mL Alkaline phosphatase stock Buffer (µL) Total volume (µL) 1 100 0.2 or 200 µL 1800 µL 2000 2 125 0.25 or 250µL 1750 µL 2000 3 150 0.3 or 300 µL 1700 µL 2000
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