VCL 4-7: Amine Formation For this assignment, the target compound that you shoul
ID: 705418 • Letter: V
Question
VCL 4-7: Amine Formation For this assignment, the target compound that you should synthesize is benzyl-disopropylamine. This is a substitution reaction. Examine the product and determine which bonds may be formed in the process Select the location of potential leaving groups Synthesis Procedures 1. Start Virtual Chemlab and select Amine Formation from the list of assignments in the electronic workbook. After entering the organic laboratory, go to the stockroom by clicking inside the Stockroom window. Next, select a round bottom flask and place it on the cork ring on the stockroom counter. Using the available reagents on the stockroom shelf, identify the appropriate starting materials required to synthesize the target compound and add them to the round bottom flask Select the appropriate solvent and click on the green Return to Lab arrow to return to the laboratory 2. The round bottom flask containing the starting materials should now be on the stir plate Click on the be in Tutorial mode and the starting materials and solvent should be listed. From the group of handle located in the upper right corner of the laboratory to pull down the TV. The TV should already reagents found on the lab bench, select the correct reagent to synthesize the target compound and add it to the flask on the stir plate 3. Start the reaction by clicking on the Stir button on the front of the stir plate. You should be able to observe the reaction mixture stirring in the flask. Monitor the progress of the reaction using TLC measurements as necessary until the product has formed and the starting materials have beern consumed. You can advance the laboratory time using the clock on the wall With the electronic lab book open (elick on the lab book on the lab bench), you can also save your TLC plates by clicking 4. When the reaction is complete, "work up" your reaction by first dragging and dropping the separatory funnel (located in a drawer) on the flask and then adding H:0 the funnel Extraci the organic layer in compound should now be in this flask List the starting materials, solvent, reagen, and products formed the funnel by elicking on the top layer and dragsing it to the cork ring on the lab hench Your targe How long did it take to finish the reaction What are the TLC valwes (R) for (a) Starting Materials Write a mechanism for this reaction (b) ProductsExplanation / Answer
The required chemicals are
1. BnCl ( Benzyl chloride)
2. Et2O
3. Isopropyl amine
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