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Chrome File Edit View History Bookmarks People Window Help 4) 880%(-1, Sun 5:07 PM 9 :E puntlandi.com | l xf (15) saed kaylie xiSaed Kaylie, 17, f xAl-Ahqaf [46:23]xBOnline quiz - CHE x Y B Take Test: Online x C Home | Chegg.co x Ochem 12A lab e x 1&step-null; Cfi -https://courses.cscc.edu/webapps/assessment/take/launch.jsp?course assessment id 4455781&course; id 1089011&content; id 7404321 E ABP Question 1 5.5 points Save Answer A student ran the following reaction and after completing the work up step, extracted the product into diethyl ether (2x10 mL). Select the correct steps for this extraction. OH 1. NaBH4 2. H+, H2 H3C H2C Step 1: Add 10 mL ether into the reaction flask. Step 1: Pour the product mixture into a separatory funnel Step 2: Add 10 mL of ether into the product mixture in the separatory funnel Step 2: Add 20 mL of ether into the product mixture in the separatory funnel Step 3: Swirl the separatory funnel with regular venting Step 3: Vigorously shake the separatory funnel until a homogenous mixture forms. Remaining Time: 1 hour, 59 minutes, 19 seconds. Question Completion Status: O Step 4: Drain the lower organic layer into a beaker O Step 4: Drain the lower aqueous layer into a beaker Step 5: Drain the remaining organic layer into a separate beaker Step 5: Drain the remaining aqueous layer into a separate beaker Step 6: Pour the organic layer back into the separatory funnel Step 6: Pour the aqueous layer back into the separatory funnel au

Explanation / Answer

step 1: pour the product mixture into the seprating flask

step 2: add 10 ml of ether into the product mixture in the separting funnel

step 3: swirl the seprating funnel with regular venting

step 4: drain the lower aqueous layer into the beaker

step 5: drain the remaining organic layer into the seprate beaker

step 6: pour the aqueous layer back into the seprating funnel

step 7: add 10 ml ether to the aqueous layer of the seprating funnel

step 8: swirl the seprating funnel with regular venting

step 9: drain the lower aqueous layer into the beaker

step 10: combine the remaining organic layer with the original organic layer that was removed

step 11: dry the organic layer with sodium sulfate

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