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What is the theoretical yield for [Mn IV (salpn)(u-O)] 2 ? The molecular weight

ID: 951138 • Letter: W

Question

What is the theoretical yield for [MnIV(salpn)(u-O)]2? The molecular weight is 702.556g

Experimental Guide:

Week 8 Experiment Guide

• Using a “double boiler” set-up, heat 50 mL of DMF [N,N-dimethylformamide] to 98- 100º C. [In a double boiler, you place your flask of DMF in a beaker of boiling water to heat it. This insures that the temperature of the DMF does not exceed the boiling point of water.]

• Add 1 mmol (0.7 g) of [MnIV(salpn)(µ-O)]2 to the hot DMF and stir until the solid is dissolved (20-30 minutes).

• Vacuum filter quickly into a clean filter flask. .

Explanation / Answer

this link will help you (1. http://chemistry.syr.edu/totah/che276/support/6a1.handouts/5.yield.pdf

2.http://socratic.org/chemistry/stoichiometry/percent-yield

3. http://editions.sciencetechnologyaction.com/lessons2-31328.php)

Recrystallization yield will be the ratio of recovered compound(pure) to the inpure compound before recrystallization. As the experimental value is not given so it is impossible to calculate percentage of yield(see 3rd link).

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