What would happen lo the purity of your product if you con led the solution loo

Question

What would happen lo the purity of your product if you con led the solution loo quickly? You are having difficulty re-crystallizing your product, so you leave the solution overnight. The following morning you have arrived to observe all of your solvent evaporated. Is your sample pure? Why or why not? What is meant by the term mother liquor? If compound A is soluble in water and ethanol at room temperature, and insoluble in dichloromethane, ether and toluene at all temperatures, how would you recrystallize an impure sample of A if you only had these five solvents available to you. Low melting solids often "oil out" of a recrystallization solution rather than crystallizing. If this to happen, how would you change the recrystallization procedure to ensure good crystals?

Explanation / Answer

24) in the purification method, slow cooling is required if you give the quock cooling all impurities are carried out with your product hence purity of your product not reached your target.

25)If your solvent evaporated, the compound never purified hence you got almost crude purity.

26) mother liquor is which is obtained from recrystallised or filtered mother liquor and mother liquor means impurities showing.

27)For this compound, the purification method is 10%ethanol in DCM(10 ml ethanol & 90 ml DCM) or 20% ethanol in DCM is best solvent just slurry at RT and filter then wash with only DCM then drying.

28)If your comound is lower melting solid then you check the boiling point if boiling point is low then go for high vacuum distillation process.other wise you set the purification method in hexane at -30 deg.

Related Questions

Navigate

• Browse (All)
• Browse W
• Subjects

---

---

Integrity-first tutoring: explanations and feedback only — we do not complete graded work. Learn more.